Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 80, Issue 10, Pages 5023-5029Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.5b00408
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Funding
- National Natural Science Foundation of China [21302048]
- Specialized Research Fund for the Doctoral Program of Higher Education [20130161120035]
- China Postdoctoral Science Foundation [2013M540625]
- Hunan Provincial Natural Science Foundation of China [14JJ7028]
- Department of Science and Technology Foundation of Changsha [k1403243-31]
- Fundamental Research Funds for the Central Universities (Hunan University)
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A copper/iron-catalyzed oxyphosphorylation of alkynes with H-phosphonates through a radical process was developed. The present protocol provides an attractive approach to beta-ketophosphonates in moderate to good yields, with the advantages of readily available substrate, high functional group tolerance and operation simplicity.
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