Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 81, Issue 1, Pages 271-275Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.5b02280
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Funding
- National Natural Science Foundation of China [21272028, 21572025, 21202013]
- Innovation AMP
- Entrepreneurship Talents Introduction Plan of Jiangsu Province
- Key University Science Research Project of Jiangsu Province [15KJA150001]
- Qing Lan Project of Jiangsu Province
- Jiangsu Key Laboratory of Advanced Catalytic Materials Technology [BM2012110]
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A TBAI-catalyzed reaction between N-tosyl hydrazone and sulfur was developed, leading to 1,2,3-thiadiazoles in moderate to good yields. It represents a facile and practical procedure to access thiadiazole under metal-free conditions. This procedure serves as an improvement for the Hurd-Mori reaction.
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