Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 80, Issue 14, Pages 6968-6975Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.5b00595
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Funding
- Special Financial Fund of Innovative Development of Marine Economic Demonstration Project [GD2012-D01-001]
- Guangdong Provincial Natural Science Foundation [S2011010001305]
- Dayawan District Science and Technology Program [201202002]
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A series of novel chiral phosphoramidite ligands based on chiral-bridged biphenyl backbones have been prepared conveniently and characterized. The ligands complexed with [IrCodCl](2) provided the first iridium catalyst system for the asymmetric addition of arylboronic acids to N-protected isatins with high efficiency. When performed in THF/H2O at 80 degrees C with 2 equiv of the arylboronic acids, the transformations acquired good to excellent results (up to 98% yield and 95% ee).
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