Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 80, Issue 9, Pages 4683-4696Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.5b00583
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Funding
- EPSRC [EP/P505534/1]
- Scottish Funding Council
- MSD
- Ministry of Higher Education and Scientific Research
- University of Benghazi, Libya
- Engineering and Physical Sciences Research Council [1097440] Funding Source: researchfish
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A one-pot multibond-forming process involving a thermally mediated Overman rearrangement and a ring closing metathesis reaction of allylic trichloroacetimidates bearing a 2-allyloxyaryl group has been developed for the synthesis Of S-amino-substituted 2,5-dihydro-1-benzoxepines. Chemoselective reduction and functionalization of these compounds allowed access to a range of pharmacologically active 5-amino-2,3,4,5-tetrahydro-1-benzoxepine scaffolds.
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