Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 80, Issue 22, Pages 11388-11397Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.5b01962
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Funding
- National Science Foundation [CHE1265964]
- National Institute of General Medical Sciences [R01-GM098601]
- Alexander von Humboldt Foundation
- NIH
- Direct For Mathematical & Physical Scien [1265964] Funding Source: National Science Foundation
- Division Of Chemistry [1265964] Funding Source: National Science Foundation
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Visible-light photoreductive coupling of 2-arylallyl bromides in the presence of the photocatalyst Ru(bpy)(3)(PF6)(2), a Hantzsch ester, and i-Pr2NEt gives 2,5-diaryl-1,5-dienes in high yield. This method avoids the use of stoichiometric metal reductants and is compatible with the presence of halogen, alkyl, electron-donating, and electron-withdrawing substituents on the aromatic ring.
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