Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 80, Issue 15, Pages 7581-7589Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.5b01177
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Funding
- National Institutes of Health (NIGMS) [R01 GM077379]
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A stereodivergent approach to the central thiolane subunit of Nuphar sesquiterpene thioalkaloids has been developed. This approach features a rhodium-catalyzed Stevens-type rearrangement in conjunction with an enzyme resolution reaction. Further elaboration into a polycyclic ring system via alcohol oxidation and ring-closing metathesis is also described.
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