Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 80, Issue 17, Pages 8887-8902Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.5b01434
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Funding
- Ministry of Science, ICT & Future Planning of Korea through the National Research Foundation of Korea [NRF-2008-2004732]
- Korea Research Institute of Chemical Technology
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Dynamic kinetic resolution driven, asymmetric transfer hydrogenation of 4-substituted cyclic sulfamidate imine-5-phosphonates produces the corresponding cyclic sulfamidate-5-phosphonates. The process employs a HCO2H/Et3N mixture as the hydrogen source and the chiral Rh catalysts, (R,R)- or (S,S)-Cp*RhCl(TsDPEN), and it takes place at room temperature within 1 h with high yields and high levels of stereoselectivity.
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