Journal
DALTON TRANSACTIONS
Volume 43, Issue 22, Pages 8461-8468Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3dt53641f
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Funding
- National Natural Science Foundation of China [21171008, 21371009, 21371010]
- Hundred Talents program of the Chinese Academy of Sciences
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SBA-15 functionalized with N-[3-(trimethoxysilyl)propyl]ethylene-diamine (TPED) was synthesized and used for the colorimetric detection of Cu2+ and removal of heavy metal ions in aqueous solutions. Compared to free SBA-15, the adsorption ability of diamine-functionalized SBA-15 (depicted as SBA-TPED) increased remarkably, the maximum adsorption capacity of SBA-TPED for Cu2+, Pb2+ and Zn2+ was 27.22, 96.43 and 12.16 mg g(-1), respectively. Furthermore, SBA-TPED exhibits high selectivity for Cu2+ with the relative selectivity coefficient of SBA-TPED for Cu2+/Pb2+ being over 10 and for Cu2+/Zn2+ being over 60. The naked-eye detection limit of SBA-TPED for Cu2+ is 0.95 ppm, and the determination of Cu2+ in real water samples also displays satisfactory results. Moreover, SBA-TPED possesses fast kinetics for removing Cu2+ with a saturation time of less than 30 min, and can be regenerated by simple acid treatment.
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