Journal
DALTON TRANSACTIONS
Volume 40, Issue 3, Pages 583-588Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c0dt01198c
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Funding
- Foundation of the National Natural Science Foundation of China [20671040, 20971054, 90922034]
- New Century Excellent Talents in University
- Chinese Ministry of Education
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Highly water-dispersible Mn3O4 nanocrystals with well-controlled size, size distribution and high crystallinity have been successfully synthesized through a modified polyol process. Poly(acrylic acid) is used as the capping agent, conferring upon the particles high water-dispersion, of which the carboxylate groups partially bind to the nanocrystal surface and the uncoordinated carboxylate groups extend into water. The water-dispersible Mn3O4 nanocrystals can be further transferred to nonpolar solvent by linking oleylamine molecules through electrostatic interaction. The as-prepared Mn3O4 nanocrystals exhibit ferromagnetic behavior at low temperature and weak paramagnetic behavior at room temperature. The Curie-Weiss temperature and the blocking temperature are 40 K and 32 K, respectively.
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