Journal
DALTON TRANSACTIONS
Volume 40, Issue 26, Pages 6984-6991Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c0dt01839b
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Funding
- Fonds der Chemischen Industrie
- Deutsche Forschungsgemeinschaft
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The tetrahydroazepine-annulated [3] ferrocenophane carbamate (4) was synthesized by two different linear routes starting from the readily available alpha-dimethylamino[3] ferrocenophane-ortho-carbaldehyde rac-6. The carbamate directed lithiation of 4 resulted in a selective attack at a (Cp)C-H bond at the higher substituted lower [3] ferrocenophane Cp-ring to eventually yield the respective ester (18) after treatment with ClCO2Me.
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