Journal
CRYSTENGCOMM
Volume 16, Issue 5, Pages 826-833Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3ce41840e
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Funding
- Human Resources Development program [20124030200130]
- Energy Technology Development program [20123021010010]
- New & Renewable Energy grant of the Korea Institute of Energy Technology Evaluation and Planning (KETEP) [20123010010160]
- Korean government's Ministry of Trade, Industry and Energy
- Korea Evaluation Institute of Industrial Technology (KEIT) [20124030200130, 20123021010010, 20123010010160] Funding Source: Korea Institute of Science & Technology Information (KISTI), National Science & Technology Information Service (NTIS)
- National Research Foundation of Korea [22A20130012456] Funding Source: Korea Institute of Science & Technology Information (KISTI), National Science & Technology Information Service (NTIS)
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Co3O4 hollow octahedra were successfully synthesized via a facile one-step solvothermal route. Time-resolved electron microscopy and X-ray diffraction analyses revealed that the Co3O4 hollow octahedra were formed through the self-assembly of primary nanocrystals followed by subsequent Ostwald ripening. Subtle control over the reaction conditions led to different morphologies (hexagonal plates and nanocubes) and crystal structures (beta-Co(OH)(2)-Co3O4 composite). The unique hollow nanostructure rendered our Co3O4 potentially useful for charge-storage applications. To prove its usefulness, the pseudocapacitive performance of the Co3O4 hollow octahedra as a supercapacitor electrode was evaluated and exhibited a charge storage capacity of 192 F g(-1) with good long-term cyclability.
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