Journal
CRYSTENGCOMM
Volume 13, Issue 12, Pages 4270-4275Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c0ce00464b
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Funding
- Korean Ministry of Education, Science and Technology [NRF-20090094026]
- World Class University [R31-2008-10029]
- National Natural Science Foundation of China [21003001]
- Ministry of Education
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TiO2 nano-octahedra and nanospheres were synthesized in toluene and ethanol solutions containing 2 mL of acetic acid and 60 mg of CTAB using a solvothermal method at 280 degrees C for 20 h. The crystalline phase of TiO2 samples was confirmed by X-ray diffraction and Raman spectroscopy. The morphology of TiO2 nanostructures was observed by scanning electron microscopy and transmission electron microscopy. The band gaps of TiO2 nano-octahedra and nanospheres were estimated from UV absorption spectra to be 3.18 and 3.23 eV. Further, due to shape-dependent properties, the TiO2 nano-octahedra show good storage performance with lithium ions when referenced to P25 TiO2.
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