Journal
CRYSTENGCOMM
Volume 13, Issue 12, Pages 4025-4031Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c0ce00629g
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Crystallisation of a glass with the composition 16Na(2)O center dot 10CaO center dot 49SiO(2)center dot 25Fe(2)O(3) led to the formation of hematite and magnetite crystals with various morphologies. Crystals containing both the hematite and the magnetite phases were detected and a strict orientation relationship between the phases is described. It is argued that hematite (Fe2O3) is the phase primarily crystallised and magnetite (Fe3O4) is the result of a phase transformation after the primary crystal growth. The main method of characterization was scanning electron microscopy (SEM) combined with electron backscatter diffraction (EBSD).
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