Journal
COMPTES RENDUS CHIMIE
Volume 15, Issue 8, Pages 719-736Publisher
ELSEVIER FRANCE-EDITIONS SCIENTIFIQUES MEDICALES ELSEVIER
DOI: 10.1016/j.crci.2012.05.003
Keywords
Sulfonic acid functionalized imidazolium salt; Ionic liquid; 14-aryl-14H-dibenzo[aj]xanthene; Tetrahydrobenzo[a]xanthene-11-one; 1,8-dioxo-octahydroxanthene; Solvent-free
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Funding
- Research Affairs Office of Bu-Ali Sina University [32-1716]
- Center of Excellence in Development of Chemical Method (CEDCM), Hamedan, I.R. Iran
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In this work, some novel sulfonic acid functionalized imidazolium salts (SAFIS), as a new category of ionic liquids, are synthesized by eco-friendly and simple procedures, and used as highly efficient and reusable catalysts to promote the following one-pot multicomponent organic transformations under solvent-free conditions: (i) the synthesis of 14-aryl-14H-dibenzo[aj]xanthenes from beta-naphthol (2 eq.) and arylaldehydes (1 eq.), (ii) the preparation of tetrahydrobenzo[a]xanthene-11-ones from beta-naphthol, arylaldehydes and dimedone, and (iii) the synthesis of 1,8-dioxo-octahydroxanthenes from dimedone (2 eq.) and aromatic aldehydes (1 eq.). Environmentally benign, simple methodologies, easy workup procedure, clean reaction, short reaction time, high yield and easy preparation of the catalysts are some advantages of this work. (C) 2012 published by Elsevier Masson SAS on behalf of Academie des sciences.
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