Journal
COMPOSITES SCIENCE AND TECHNOLOGY
Volume 86, Issue -, Pages 9-17Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.compscitech.2013.06.017
Keywords
Fibers; Nano composites; Particle-reinforced composites; Scanning electron microscopy (SEM); Scanning/transmission electron microscopy (STEM); Electro-spinning
Categories
Funding
- Department of Science and Technology, Government of India
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ZnO nanorods with high aspect ratio were synthesized and were dispersed in poly(vinyl alcohol) (PVA)water, PVA-water-N,N-dimethylforamide (DMF) and poly(acrylonitrile) (PAN)-DMF systems. These mixtures were electrospun to understand their spinning behaviour. It was found that only PAN-DMF system could result in formation of nanofiber composites reinforced with aligned ZnO rods. PAN nanofibers reinforced with ZnO rods up to 50 wt% on the weight of polymer could be readily electrospun. The presence of aligned ZnO rods inside PAN nanofibers was confirmed using scanning electron microscopy (SEM) and scanning/transmission electron microscopy (STEM). Raman analysis revealed that such reinforced nano-composites are enabled only when ZnO rods could interact with both the dispersant as well as the polymer. Both random and aligned ZnO-PAN reinforced nanofibers could be successfully produced to suit different applications. (C) 2013 Elsevier Ltd. All rights reserved.
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