Journal
JOURNAL OF MAGNETIC RESONANCE
Volume 253, Issue -, Pages 60-70Publisher
ACADEMIC PRESS INC ELSEVIER SCIENCE
DOI: 10.1016/j.jmr.2014.12.019
Keywords
Sedimentation; Solid State NMR; Sample preparation; DNP; Bioinspired materials; NMR crystallography
Funding
- MIUR PRIN [2012SK7ASN]
- EC Contract Bio-NMR [261863]
- Instruct, European Strategy Forum on Research Infrastructures (ESFRI)
- EMBO
- Ente Cassa di Risparmio di Firenze
- EC Contract pNMR [317127]
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Resolution and sensitivity in solid state NMR (SSNMR) can rival the results achieved by solution NMR, and even outperform them in the case of large systems. However, several factors affect the spectral quality in SSNMR samples, and not all systems turn out to be equally amenable for this methodology. In this review we attempt at analyzing the causes of this variable behavior and at providing hints to increase the chances of experimental success. (C) 2015 Elsevier Inc. All rights reserved.
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