Journal
JOURNAL OF MAGNETIC RESONANCE
Volume 252, Issue -, Pages 170-175Publisher
ACADEMIC PRESS INC ELSEVIER SCIENCE
DOI: 10.1016/j.jmr.2015.01.006
Keywords
Heteronuclear coupling constants; IPAP; HSQMBC; Multiplicity-editing; HOBS
Funding
- MINECO of Spain [CTQ2012-32436]
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Even C/CH2 and odd CH/CH3 carbon-multiplicity information can be directly distinguished from the relative positive/negative phase of cross-peaks in a novel ME (Multiplicity-Edited)-selHSQMBC experiment. The method can be extended by a TOCSY propagation step, and it is fully compatible for the simultaneous and precise determination of long-range heteronuclear coupling constants. Broadband homonuclear decoupling techniques can also be incorporated to enhance sensitivity and signal resolution by effective collapse of J(HH) multiplets. (C) 2015 Elsevier Inc. All rights reserved.
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