Journal
CHINESE JOURNAL OF CHEMISTRY
Volume 30, Issue 8, Pages 1797-1800Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/cjoc.201200264
Keywords
phosphorylation of alcohols; B(C6F5)3; phosphate esters
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Funding
- Fundamental Research Funds for the Lanzhou University [lzu-jbky-2011-136]
- Natural Science Foundation for Young Scientists in Gansu Province, China [1107RJYA038]
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The phosphoryl transfer reactions of diphenyl chlorophosphate with a wide range of alcohols were catalyzed by tris(pentafluorophenyl)boron [B(C6F5)3], giving the corresponding phosphate esters in excellent yields. This methodology has advantages over older ones because it employs the easily handled B(C6F5)3, avoids the side reaction, and has shorter reaction time.
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