Journal
CHINESE CHEMICAL LETTERS
Volume 25, Issue 1, Pages 87-89Publisher
ELSEVIER SCIENCE INC
DOI: 10.1016/j.cclet.2013.09.003
Keywords
Thiourea nitrate; Nitration; Thiourea; Aromatic compounds
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Funding
- Fundamental Research Funds for the Central Universities
- Scientific Research Foundation for the Returned Overseas Chinese Scholars, State Education Ministry, PR China
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Thiourea nitrate (TN) was easily prepared from thiourea and nitric acid to explore its use as a new nitration reagent. Nitrations of various aromatic compounds utilizing TN in concentrated sulfuric acid were studied. TN could convert aromatic compounds to the corresponding nitrated derivatives with various abnormal yields under mild conditions. The results suggested that the reaction mechanism might be different from those of traditional nitration reagents. (C) 2013 Juan Shi. Published by Elsevier B.V. on behalf of Chinese Chemical Society. All rights reserved.
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