Journal
CHINESE CHEMICAL LETTERS
Volume 21, Issue 12, Pages 1411-1414Publisher
ELSEVIER SCIENCE INC
DOI: 10.1016/j.cclet.2010.06.019
Keywords
In situ nanocatalysis; Palladium nanoparticles; Heck reaction; Polyethylene glycol
Categories
Funding
- State Key Laboratory of Fine Chemicals [KF0801]
- Science Research Foundation of DUT
- DUT
- National Natural Science Foundation of China [20976024]
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A ligand-free Heck reaction catalyzed by in situ-generated palladium nanoparticles in PEG-400 has been developed. This catalytic system is a simple and active protocol for the Heck reaction of aryl halides under mild conditions. Comparative experiments demonstrated that the Heck reaction catalyzed by the palladium nanoparticles in situ-generated under the Heck reaction conditions was carried out much quicker than that by the in ex situ-generated ones. (C) 2010 Chun Liu. Published by Elsevier B.V. on behalf of Chinese Chemical Society. All rights reserved.
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