4.7 Article

Step-wise sequential phase partition (SSPP) algorithm based statistical modeling and online process monitoring

Journal

CHEMOMETRICS AND INTELLIGENT LABORATORY SYSTEMS
Volume 125, Issue -, Pages 109-120

Publisher

ELSEVIER
DOI: 10.1016/j.chemolab.2013.03.017

Keywords

Multiphase batch processes; Sequential phase partition; Transition patterns; Online process monitoring; Multivariate statistical analysis

Funding

  1. Program for New Century Excellent Talents in University [NCET-12-0492]
  2. National Natural Science Foundation of China [61273166]
  3. Specialized Research Fund for the Doctoral Program of Higher Education of China [20120101120182]
  4. Fundamental Research Funds for the Central Universities [2012QNA5012]
  5. Project of Education Department of Zhejiang Province [Y201223159]
  6. Technology Foundation for Selected Overseas Chinese Scholar of Zhejiang Province
  7. Foundation of Key Laboratory of System Control and Information Processing, Ministry of Education, P.R China

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As batches operate at different statuses across different phases, it can be advantageous to partition the whole batch process into different phases and characterize them separately by multiple phase models. The conventional clustering-based division algorithm overlooks the time sequence of process phases and it is hard to capture the transition patterns between neighboring phases. In the present work, an automatic step-wise sequential phase partition (SSPP) algorithm is developed, which can capture the changes of process characteristics by checking their influences on monitoring system. Its theoretical support and the related statistical characteristics are analyzed. Using this algorithm, major phases are captured and also distinguished from transition patterns. The time-varying characteristics are thus described by different statistical models. For online application, the affiliation of each new sample can be realtime judged and its status can be checked by adopting the proper statistical model. Comparison is conducted between the proposed algorithm and clustering-based phase division algorithm. Comprehensive analyses are made regarding the influences of important parameters on monitoring performance. The proposed method is illustrated by a three-tank experimental system and an injection molding process which both present typical multiphase nature and transition characteristics. (C) 2013 Elsevier B.V. All rights reserved.

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