Journal
CHEMISTRY-A EUROPEAN JOURNAL
Volume 20, Issue 42, Pages 13811-13814Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/chem.201403275
Keywords
acylation; green chemistry; ketones; organocatalysis; photochemistry
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Funding
- Education and Lifelong Learning operational program through NSRF ENISigmaXYSigmaH METADeltaIDeltaAKTOPOmegaN EREYNHTOmegaN program - ESF [PE 2431]
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A fast and efficient visible-light metal-free hydroacylation of dialkyl azodicarboxylates is described. Among a variety of activated ketones, phenyl glyoxylic acid and its ethyl ester were identified as suitable photoorganocatalysts. A range of aliphatic and aromatic aldehydes were employed, thus leading to products in high to excellent yields.
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