Journal
CHEMISTRY-A EUROPEAN JOURNAL
Volume 20, Issue 1, Pages 58-63Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/chem.201303802
Keywords
amines; deuterium labelling; DMSO; formic acid; methylation
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Funding
- National Science Foundation of China [21103102]
- Program for Changjiang Scholars and Innovative Research Team in University [IRT 1070]
- Cheung Kong Scholar Programme
- Fundamental Research Funds for the Central Universities [GK261001095]
- Program for Key Science and Technology Innovative Team of Shaanxi Province [2012KCT-21, 2013KCT-17]
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DMSO methylates a broad range of amines in the presence of formic acid, providing a novel, green and practical method for amine methylation. The protocol also allows the one-pot transformation of aromatic nitro compounds into dimethylated amines in the presence of a simple iron catalyst.
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