Journal
CHEMISTRY-A EUROPEAN JOURNAL
Volume 19, Issue 24, Pages 7809-7816Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/chem.201204638
Keywords
crystal engineering; density functional calculations; metal-organic frameworks; self-assembly; X-ray absorption spectroscopy
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Funding
- U.S. Department of Energy, Office of Science, Office of Basic Energy Sciences [DE-AC02-98CH10886]
- Technology Foundation STW
- National Science Foundation NWO
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We present an in situ small- and wide-angle X-ray scattering (SAXS/WAXS) and quick-scanning extended X-ray absorption fine-structure (QEXAFS) spectroscopy study on the crystallization of the metal-organic framework ZIF-7. In combination with DFT calculations, the self-assembly and growth of ZIF-7 microrods together with the chemical function of the crystal growth modulator (diethylamine) are revealed at all relevant length scales, from the atomic to the full crystal size.
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