Journal
CHEMISTRY OF HETEROCYCLIC COMPOUNDS
Volume 47, Issue 12, Pages 1561-1564Publisher
SPRINGER
DOI: 10.1007/s10593-012-0948-8
Keywords
6-sulfamoylsaccharin; alkylation; benzylation; oxidative cyclization; regioselectivity
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Funding
- European Social Fund [2009/0203/1DP/1.1.1.2.0/APIA/VIAA/023]
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An improved method for the preparation of 6-sulfamoylsaccharin (3-oxo-2,3-dihydro-1,2-benzo-thiazole-6-sulfonamide 1,1-dioxide) has been developed and studies of its possible direct alkylation have been carried out. It was shown that alkylation occurs regioselectively at the isothiazoline ring nitrogen atom.
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