Journal
CHEMISTRY LETTERS
Volume 42, Issue 11, Pages 1435-1437Publisher
CHEMICAL SOC JAPAN
DOI: 10.1246/cl.130726
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Funding
- Japan Science and Technology Agency (JST)
- Core Research for Evolutional Science and Technology (CREST) project
- Ministry of Education, Culture, Sports, Science and Technology of Japan
- Grants-in-Aid for Scientific Research [11J09752] Funding Source: KAKEN
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Li2S-P2S5 solid electrolyte (SE) powders were successfully reprecipitated from a liquid phase. Powders of 80Li(2)S center dot 20P(2)S(5) (mol %) SE originally prepared by mechanical milling were dissolved in N-methylformamide (NMF) and a homogeneous solution was obtained. The NMF solution was dried at 150 degrees C for 3 h under vacuum to obtain precipitates. The main structural unit in the obtained powder was PS43-. The crystalline phase of the powders was confirmed to be Li3PS4, and ionic conductivity was 2.6 x 10(-6) cm(-1).
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