Journal
CHEMISTRY LETTERS
Volume 41, Issue 4, Pages 432-434Publisher
CHEMICAL SOC JAPAN
DOI: 10.1246/cl.2012.432
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Funding
- UGC, India
- CSIR, India
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A simple protocol for the alpha-monochlorination of ketones and 1,3-dicarbonyl compounds utilizing NH4Cl as a source of chlorine and Oxone as an oxidant in methanol without catalyst is presented. The reaction proceeds at ambient temperature in yields ranging from moderate to excellent.
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