Journal
CHEMISTRY LETTERS
Volume 38, Issue 2, Pages 166-167Publisher
CHEMICAL SOC JAPAN
DOI: 10.1246/cl.2009.166
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Tris(bipyridyl)ruthenium(II) ([Ru(bpy)(3)](2+) : TB(II)) catalyzes oxidative coupling of enamines and aldehydes with 2,2,6,6-tetramethylpiperidinyl-1-oxy (TEMPO) under irradiation of visible light to afford alpha-oxyaminated carbonyl compounds. The visible light irradiation is essential to generate the triplet excited state of *TB(II) which acts as an oxidizing agent. This is a new procedure for radical coupling based on single electron transfer mediated by photoactivated TB.
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