Journal
CHEMISTRY LETTERS
Volume 38, Issue 5, Pages 458-459Publisher
CHEMICAL SOC JAPAN
DOI: 10.1246/cl.2009.458
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Funding
- Ministry of Education, Culture, Sports, Science and Technology, Industrial Technology Research
- NEDO of Japan
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Aryl 1-thioglycosides have directly been synthesized in good yields from the corresponding unprotected sugars and thiols without protection of the hydroxy groups by using 2-chloro-1,3-dimethylimidazolinium chloride (DMC) as dehydrative condensing agent. The reaction proceeded in a mixed solvent of water and acetonitrile under mild reaction conditions, leading to the predominant formation of beta-anomers.
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