Journal
CHEMISTRY LETTERS
Volume 37, Issue 9, Pages 942-943Publisher
CHEMICAL SOC JAPAN
DOI: 10.1246/cl.2008.942
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Funding
- JSPS [18750085, 17205012, 20245008]
- Global COE program from the MEXT, Japan
- Grants-in-Aid for Scientific Research [17205012, 18750085, 20245008] Funding Source: KAKEN
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We have found that tetrabutylammonium triflate (Bu4NOTf) serves as an effective electrolyte for electrochemical glycosylation Using thioglycosides. Based on this method, a one-pot electrochemical glycosylation-Fmoc group deprotection sequence has been developed. This sequence has been successfully applied to the synthesis of a pentasaccharide.
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