Journal
CHEMICAL ENGINEERING JOURNAL
Volume 165, Issue 2, Pages 405-412Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/j.cej.2010.08.068
Keywords
Synthesis; Organic-inorganic hybrid material; Toxic metals and environmental applications
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Funding
- Council of Science and Technology, Lucknow, U.P. [CST/D-3554]
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A composite cation exchange material n-butylacetatezirconium(IV) iodate was prepared under different experimental conditions. Ion-exchange material synthesized at pH 0.8 shows an ion-exchange capacity of 1.8 meq g(-1) for Na+ ions. The material has been characterized on the basis of X-ray, TGA, FTIR, SEM, AFM and Raman studies. Ion-exchange capacity, pH titration, elution behavior and distribution studies were also carried out to determine the preliminary ion-exchange properties of the material. The effect of temperature on the ion-exchange capacity of the material has also been studied. The sorption behavior towards metal ions was studied in ethyl acetate, DMF. DMSO and H3PO4 systems. A few quantitative binary separations of metal ions on the column, packed with this material has been achieved to establish its usefulness as ion-exchanger. The practical utility of n-butylacetatezirconium(IV) iodate cation exchanger has been established to recover toxic metals from environmental wastes. (C) 2010 Published by Elsevier B.V.
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