Journal
CHEMICAL ENGINEERING & TECHNOLOGY
Volume 32, Issue 11, Pages 1695-1701Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ceat.200900369
Keywords
Capillary microreactor; Diels-Alder reaction; Miniaturization; Supercritical fluids
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Recent examples of high-pressure organic reactions in (flow) glass microreactors of micrometer dimensions are described. Different types of reactions such as Diels-Alder and nucleophilic aromatic substitution reactions performed in a capillary microreactor gave rate enhancements of 1.5-2.7 at 600 bar. Specifically designed flow glass microreactors, that withstand pressures of 140-690 bar, were used to Study Diels-Alder and oxidation reactions. The use of supercritical fluids gives rise to considerable rate enhancements, while the use of a transparent microreactor allows to visualize phase transitions.
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