Journal
CHEMICAL COMMUNICATIONS
Volume 50, Issue 29, Pages 3865-3867Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c4cc01053a
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Funding
- National Natural Science Foundation of China [21272028, 21202013]
- Innovation & Entrepreneurship Talents'' Introduction Plan of Jiangsu Province
- Natural Science Foundation of Zhejiang Province [R4110294]
- Jiangsu Key Laboratory of Advanced Catalytic Materials Technology
- State Key Laboratory of Coordination Chemistry at Nanjing University
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An FeCl2-promoted carbomethylation of arylacrylamides by di-tert-butyl peroxide (DTBP) is achieved, leading to 3-ethyl-3-substituted indolin-2-one in high yield. The reaction tolerates a series of functional groups, such as cyano, nitro, ethyloxy carbonyl, bromo, chloro, and trifluoromethyl groups. The radical methylation and arylation of the alkenyl group are involved in this reaction.
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