Journal
CHEMICAL COMMUNICATIONS
Volume 50, Issue 39, Pages 5014-5016Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c4cc01305k
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An oxidation of allylic and benzylic alcohols to the corresponding carboxylic acids is effected by merging a Cu-catalyzed oxidation using O-2 as a terminal oxidant with a subsequent chlorite oxidation (Lindgren oxidation). The protocol was optimized to obtain pure products without chromatography or crystallization. Interception at the aldehyde stage allowed for Z/E-isomerization, thus rendering the oxidation stereoconvergent with respect to the configuration of the starting material.
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