Journal
CHEMICAL COMMUNICATIONS
Volume 49, Issue 81, Pages 9263-9265Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3cc44792h
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The air and moisture stable fluoroiodane 8, readily prepared on a 6 g scale by nucleophilic fluorination of the hydroxyiodane 7 with TREAT-HF, has been used as an electrophilic fluorinating reagent for the first time to monofluorinate 1,3-ketoesters and difluorinate 1,3-diketones in good isolated yields.
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