Journal
CHEMICAL COMMUNICATIONS
Volume 49, Issue 81, Pages 9344-9346Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3cc45175e
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Funding
- Department of Science and Technology, Council of Scientific and Industrial Research and University Grants Commission New Delhi (India)
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The PdTe NPs (hexagonal) and nanorods (first example) have been synthesized for the first time from single source precursors (SSPs), [Pd(L1)Cl-2] (1) and [Pd(L2)Cl]BF4 (2) [L1, 4-bromo-1-[2-(4-methoxyphenyltellanyl)ethyl]-1H-pyrazole; L2, bis-[2-(4-bromopyrazol-1-yl)ethyl]telluride], by their thermolysis in an OA-ODE mixture (1 : 1) and TOP respectively. The composition of the PdTe phase does not change with SSP/solvent. Complex 2 gives small size nanostructures.
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