Journal
CHEMICAL COMMUNICATIONS
Volume 49, Issue 70, Pages 7735-7737Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3cc44422h
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- NIGMS NIH HHS [R01 GM076125] Funding Source: Medline
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Several cycloaddition catalysts and reagents were surveyed for their effectiveness toward cyclizing alkynenitriles with cyanamides. Catalytic amounts of FeI2, (iPr)PDAI and Zn were found to effectively catalyze the [2+2+2] cycloaddition of a variety of cyanamides and alkynenitriles to afford bicyclic 2-aminopyrimidines.
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