Journal
CHEMICAL COMMUNICATIONS
Volume 49, Issue 98, Pages 11518-11520Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3cc46049e
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Funding
- US Department of Energy, Industrial Technologies Program [NT08847, DE-AC-05-RL01830]
- DOE-ARPA-E Navy matching grant
- ONAMI matching grant
- Oregon BEST equipment grants
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The reaction conditions for the synthesis of Cu-BTC (BTC = benzene-1,3,5-tricarboxylic acid) were elucidated using a continuous-flow microreactor-assisted solvothermal system to achieve crystal size and phase control. A high-rate synthesis of Cu-BTC metal-organic frameworks with a BET surface area of more than 1600 m(2) g(-1) (Langmuir surface area of more than 2000 m(2) g(-1)) and with a 97% production yield could be achieved with a total reaction time of 5 minutes.
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