Journal
CHEMICAL COMMUNICATIONS
Volume 49, Issue 32, Pages 3342-3344Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3cc40541a
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Funding
- CSIR (as part of NCL-IGIB joint research collaboration program)
- UGC
- CSIR
- Multi-scale simulation and Modeling project - MSM
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Concise and protecting-group free synthesis of ent-palmyrolide A and (-)-cis-palmyrolide A were achieved starting from commercially available (S)-citronellal. The key fragment of palmyrolide A, (5S,7S)-7-hydroxy-5,8,8-trimethylnonanamide'', which makes up the most challenging part of the target molecule, was prepared in just three steps. A plausible mechanism for the trans-cis isomerization of the double bond in the macrocycle has been investigated.
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