Journal
CHEMICAL COMMUNICATIONS
Volume 49, Issue 95, Pages 11206-11208Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3cc46544f
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Funding
- Platform for Drug Discovery, Informatics, and Structural Life Science from the Ministry of Education, Culture, Sports, Science and Technology, Japan
- MEXT (Ministry of Education, Culture, Sports, Science and Technology) [24105513, 2304]
- JST (ACT-C: Creation of Advanced Catalytic Transformation for the Sustainable Manufacturing at Low Energy, Low Environmental Load)
- Grants-in-Aid for Scientific Research [24655048] Funding Source: KAKEN
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A catalytic enantioselective monofluoromethylation of aldehydes using 2-fluoro-1,3-benzodithiole-1,1,3,3-tetraoxide (FBDT) was realized. With a bifunctional thiourea-titanium catalytic system, the monofluoromethylated- adducts were obtained in good yields and high enantioselectivities, up to 96% ee.
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