Journal
CHEMICAL COMMUNICATIONS
Volume 48, Issue 5, Pages 654-656Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c1cc15242d
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Funding
- EQUIPEX [ANR-10-EQPX-47-01]
- EU [PIIF-GA-2010-274574]
- ETH Zurich
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A series of non-aqueous solvents combined with the exogenous biradical bTbK are developed for DNP NMR that yield enhancements comparable to the best available water based systems. 1,1,2,2-tetrachloroethane appears to be one of the most promising organic solvents for DNP solid-state NMR. Here this results in a reduction in experimental times by a factor of 1000. These new solvents are demonstrated with the first DNP surface enhanced NMR characterization of an organometallic complex supported on a hydrophobic surface.
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