Journal
CHEMICAL COMMUNICATIONS
Volume 48, Issue 35, Pages 4244-4246Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c2cc31007d
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In the present work, we demonstrate the feasibility to form an aligned Nb2O5 nanotube layer by self-organizing anodization of Nb in a NH4F-glycerol electrolyte. In order to achieve a nanotubular rather than a nanoporous layer, careful optimization of the anodization electrolyte is required. We show that only in a narrow window of electrolyte parameters highly aligned nanotubes of 50 nm inner diameter and several micrometres in length can be formed.
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