Journal
CHEMICAL COMMUNICATIONS
Volume 48, Issue 10, Pages 1434-1436Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c1cc12932e
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Funding
- ANR [ANR-09-PIRIBio-445583]
- CONACYT
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An efficient synthetic route is proposed to produce 2-hydroxy-2-ethyl-3-oxobutanoate for the specific labelling of Ile methyl-gamma(2) groups in proteins. The H-2, C-13-pattern of the biosynthetic precursor has been designed to optimize magnetization transfer, in large proteins, between these important structural probes and their corresponding backbone nuclei.
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