Journal
CHEMICAL COMMUNICATIONS
Volume 48, Issue 62, Pages 7747-7749Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c2cc33611a
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Funding
- Division Of Chemistry
- Direct For Mathematical & Physical Scien [936862] Funding Source: National Science Foundation
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A very short synthesis (5 steps), the crystal structure and resolution of an elaborate, inherently chiral [n](1,6)pyrenophane is reported. The synthesis hinges upon two very productive events: a multicomponent reaction and an unprecedented double-McMurry/valence isomerization/dehydrogenation step. Aromatization reactions are involved in the formation of all four of the rings of the pyrene system.
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