Journal
CHEMICAL COMMUNICATIONS
Volume 48, Issue 79, Pages 9828-9830Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c2cc34689c
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Funding
- National Science Foundation Graduate Research Fellowship Program (NSF-GRFP)
- U.S. Department of Energy [DE-SC0004888]
- U.S. Department of Energy (DOE) [DE-SC0004888] Funding Source: U.S. Department of Energy (DOE)
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The synthesis and successful activation of IRMOF-8 (Zn4O(ndc)(3), ndc = naphthalene-2,6-dicarboxylate) is presented. Room temperature synthesis effectively suppresses interpenetration. Although conventional activation under reduced pressure leads to structural collapse, activation by flowing supercritical CO2 yields a guest-free material with a BET surface area of 4461 m(2) g(-1).
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