Journal
CHEMICAL COMMUNICATIONS
Volume 48, Issue 23, Pages 2876-2878Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c2cc17332h
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Funding
- American Chemical Society [46587-G3]
- University of Iowa
- Division Of Chemistry
- Direct For Mathematical & Physical Scien [0946779] Funding Source: National Science Foundation
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An (alkene) peroxoiridium(III) complex, [Ir(L)(cod)(O-2)] [where LH = PhN=C(NMe2)NHPh and cod = 1,5-cyclooctadiene], was identified as an intermediate in the reaction of the Ir I precursor [Ir(L)(cod)] with O2 and characterized by spectroscopic methods. Decay of the intermediate and further reaction with 1,5-cyclooctadiene produced 4-cycloocten-1-one.
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