Journal
CHEMICAL COMMUNICATIONS
Volume 48, Issue 79, Pages 9930-9932Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c2cc34787c
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Funding
- Gobierno Vasco [IT477-10]
- Universidad del Pais Vasco/Euskal Herriko Unibertsitatea [UFI 11/53]
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The direct acid-base reaction between ZnO/CoO/Co(OH)(2) and imidazolic ligands under moderate heating (100-160 degrees C), in a closed vessel, leads to the generation of the corresponding zinc/cobalt-imidazolates in a high yield (87-97%) in which network topology is controlled by the addition of small amounts of structure directing agents. Moreover, the fine tuning of the thermal process at the synthetic stage permits us to increase the crystal size, and even to grow X-ray quality single crystals.
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