Journal
CHEMICAL COMMUNICATIONS
Volume 48, Issue 35, Pages 4250-4252Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c2cc30391d
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Funding
- MEST of the Korean Government through the National Research Foundation [NRF-2011-C1AAA001-2011-0030278]
- Korea Center for Artificial Photosynthesis (KCAP) in Sogang University
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We report a novel method for synthesizing monodisperse mesoporous TiO2 spheres (sizes = 0.6-3.1 mu m) by hydrolysis of titanium isopropoxide (TIP) in a mixture of C-8-C-16 n-alkylamine, water, and ethanol. The size increases with decreasing temperature, TIP concentration, and water concentration, and upon purifying TIP. n-Dodecylamine gives the highest monodispersity.
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