Journal
CHEMICAL COMMUNICATIONS
Volume 47, Issue 23, Pages 6593-6595Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c1cc10678c
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Solutions of aza-Morita-Baylis-Hillman (aza-MBH) reactions were directly monitored by ESI(+)-MS(/MS) spectrometry to obtain information on their mechanism. A unique bis-sulfonamide intermediate was intercepted and characterized and, based on this novel species, a mechanism that rationalizes the uniqueness of aza-MBH reactions is proposed.
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