Journal
CHEMICAL COMMUNICATIONS
Volume 47, Issue 38, Pages 10827-10829Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c1cc14602e
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Funding
- Priority Academic Program Development of Jiangsu Higher Education Institutions (PAPD)
- NSFC [20802047, 21072142]
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A new tert-butyl peresters synthesis directly from aldehydes and TBHP was developed via Bu4NI-catalyzed aldehyde C-H oxidation. Mechanistic studies suggest that the protocol proceeds via a radical process. Combining the method with the Kharasch-Sosnovsky reaction offers a practical approach for the synthesis of allylic esters from simple aldehydes and alkenes via a two-step one-pot procedure.
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